Processing, characterization, and mechanical properties of beta silicon nitride whisker/silicon nitride matrix composites
Neergaard, Lynn James
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https://hdl.handle.net/2142/23242
Description
Title
Processing, characterization, and mechanical properties of beta silicon nitride whisker/silicon nitride matrix composites
Author(s)
Neergaard, Lynn James
Issue Date
1990
Doctoral Committee Chair(s)
Homeny, J.
Department of Study
Applied Mechanics
Engineering, Materials Science
Discipline
Applied Mechanics
Engineering, Materials Science
Degree Granting Institution
University of Illinois at Urbana-Champaign
Degree Name
Ph.D.
Degree Level
Dissertation
Keyword(s)
Applied Mechanics
Engineering, Materials Science
Language
eng
Abstract
Ceramic matrix composites, consisting of $\beta$-$\rm Si\sb3N\sb4$ whisker reinforced polycrystalline $\rm Si\sb3N\sb4$, were fabricated with controlled whisker/matrix interfaces, characterized on the microstructural level, and evaluated for mechanical reliability. As-received and coated $\beta$-$\rm Si\sb3N\sb4$ whiskers were used to reinforce the $\rm Si\sb3N\sb4$ matrices. Whisker coatings were achieved by low pressure chemical vapor deposition of BN. As-received and coated whiskers and as-received powders were characterized using XRD, XPS, SEM, and TEM techniques. Composite microstructures, including the whisker/matrix interfacial zones, were characterized by SEM and TEM. Mechanical properties of the composites, primarily fracture strength and fracture toughness, were measured and compared to those of the unreinforced matrices.
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